Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-3 |
Synchrotron site | ESRF |
Beamline | ID14-3 |
Temperature [K] | 287 |
Detector technology | CCD |
Collection date | 1999-06-16 |
Detector | MARRESEARCH |
Spacegroup name | H 3 2 |
Unit cell lengths | 288.000, 288.000, 653.000 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 26.140 - 2.560 |
R-factor | 0.197 |
Rwork | 0.197 |
R-free | 0.20300 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | MS2 RECOMBINANT CAPSIDS |
RMSD bond length | 0.008 |
RMSD bond angle | 1.400 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | CNS (1.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.650 |
High resolution limit [Å] | 2.560 | 2.560 |
Rmerge | 0.180 | 0.370 |
Number of reflections | 254630 | |
Completeness [%] | 77.0 | 8 |
Redundancy | 3.8 | 1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.4 | pH 7.40 |