Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | MAX II BEAMLINE I711 |
Synchrotron site | MAX II |
Beamline | I711 |
Temperature [K] | 280 |
Detector technology | CCD |
Collection date | 2001-03-24 |
Detector | MARRESEARCH |
Spacegroup name | H 3 2 |
Unit cell lengths | 288.000, 288.000, 653.000 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 38.240 - 2.700 |
R-factor | 0.246 |
Rwork | 0.246 |
R-free | 0.24300 |
Structure solution method | OTHER |
RMSD bond length | 0.007 |
RMSD bond angle | 1.400 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | CNS (1.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 2.800 |
High resolution limit [Å] | 2.700 | 2.700 |
Rmerge | 0.210 | |
Number of reflections | 134487 | |
Completeness [%] | 48.3 | 9.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | other * | 7.4 | Valegard, K., (1986) J. Mol. Biol., 190, 587. * |