2IZ5
FUNCTION AND STRUCTURE OF THE MOLYBDENUM COFACTOR CARRIER PROTEIN MCP FROM CHLAMYDOMONAS REINHARDTII
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BESSY BEAMLINE 14.1 |
Synchrotron site | BESSY |
Beamline | 14.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-07-15 |
Detector | MARRESEARCH |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 68.313, 75.881, 126.631 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 65.090 - 2.290 |
R-factor | 0.218 |
Rwork | 0.215 |
R-free | 0.27300 |
Structure solution method | SAD |
RMSD bond length | 0.019 |
RMSD bond angle | 1.918 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.480 |
High resolution limit [Å] | 2.380 | 2.380 |
Rmerge | 0.060 | 0.330 |
Number of reflections | 53717 | |
<I/σ(I)> | 22.6 | 2.3 |
Completeness [%] | 94.5 | 88.1 |
Redundancy | 3.7 | 3.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 8 | pH 8.00 |