2IYN
The co-factor-induced pre-active conformation in PhoB
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | EMBL/DESY, HAMBURG BEAMLINE BW7A |
Synchrotron site | EMBL/DESY, HAMBURG |
Beamline | BW7A |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | MARRESEARCH |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 50.742, 105.829, 135.510 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.000 - 2.080 |
R-factor | 0.233 |
Rwork | 0.231 |
R-free | 0.30500 |
Structure solution method | OTHER |
RMSD bond length | 0.016 |
RMSD bond angle | 1.503 |
Refinement software | REFMAC (5.1.24) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 45.200 |
High resolution limit [Å] | 2.080 |
Rmerge | 0.080 |
Number of reflections | 20372 |
<I/σ(I)> | 5.2 |
Completeness [%] | 91.4 |
Redundancy | 5.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |