2IXT
SPHERICASE
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | EMBL/DESY, HAMBURG BEAMLINE BW7B |
Synchrotron site | EMBL/DESY, HAMBURG |
Beamline | BW7B |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2000-09-18 |
Detector | MARRESEARCH |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 46.088, 62.668, 84.874 |
Unit cell angles | 90.00, 95.47, 90.00 |
Refinement procedure
Resolution | 84.520 - 0.800 |
R-factor | 0.138 |
Rwork | 0.137 |
R-free | 0.15400 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ea7 |
RMSD bond length | 0.014 |
RMSD bond angle | 1.613 |
Data reduction software | MOSFLM |
Phasing software | AMoRE |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 84.500 | |
High resolution limit [Å] | 0.800 | |
Rmerge | 0.050 | |
Number of reflections | 411650 | |
<I/σ(I)> | 6.5 | 1.8 |
Completeness [%] | 81.0 | |
Redundancy | 2.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.5 | pH 7.5 |