2IXK

RmlC P aeruginosa with dTDP-4-keto rhamnnose (the product of the reaction)

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SRS BEAMLINE PX9.5
Synchrotron site	SRS
Beamline	PX9.5
Temperature [K]	100
Detector technology	CCD
Detector	MARRESEARCH
Spacegroup name	P 21 21 2
Unit cell lengths	64.378, 146.208, 44.919
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	72.550 - 1.700
R-factor	0.152
Rwork	0.150
R-free	0.19800
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.011
RMSD bond angle	1.420
Data reduction software	MOSFLM
Data scaling software	SCALA
Refinement software	REFMAC (5.2.0007)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	21.000	1.800
High resolution limit [Å]	1.700	1.700
Rmerge	0.080	0.380
Number of reflections	40067
<I/σ(I)>	5.6	1.8
Completeness [%]	84.0	40
Redundancy	6.1	4.7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1