2IWX
Analogues of radicicol bound to the ATP-binding site of Hsp90.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-1 |
Synchrotron site | ESRF |
Beamline | ID14-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-02-19 |
Detector | ADSC CCD |
Spacegroup name | P 43 2 2 |
Unit cell lengths | 73.703, 73.703, 110.019 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 73.720 - 1.500 |
R-factor | 0.2 |
Rwork | 0.198 |
R-free | 0.23600 |
Structure solution method | OTHER |
RMSD bond length | 0.012 |
RMSD bond angle | 1.591 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 1.580 |
High resolution limit [Å] | 1.500 | 1.500 |
Rmerge | 0.080 | 0.250 |
Number of reflections | 49255 | |
<I/σ(I)> | 23.3 | 6.4 |
Completeness [%] | 100.0 | 100 |
Redundancy | 8.5 | 6.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |