2IVM
Crystal structure of a transcriptional regulator
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 298 |
Detector technology | IMAGE PLATE |
Detector | MARRESEARCH |
Spacegroup name | P 42 21 2 |
Unit cell lengths | 100.827, 100.827, 99.503 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.070 - 2.500 |
R-factor | 0.201 |
Rwork | 0.199 |
R-free | 0.25500 |
Structure solution method | MIRAS |
RMSD bond length | 0.026 |
RMSD bond angle | 2.584 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | SOLVE |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.640 |
High resolution limit [Å] | 2.500 | 2.500 |
Rmerge | 0.100 | 0.650 |
Number of reflections | 18352 | |
<I/σ(I)> | 19.2 | 4.5 |
Completeness [%] | 99.9 | 100 |
Redundancy | 9.1 | 9.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.5 | pH 6.5 |