2IU6
REGULATION OF THE DHA OPERON OF LACTOCOCCUS LACTIS
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU300 |
Temperature [K] | 110 |
Detector technology | IMAGE PLATE |
Detector | RIGAKU RAXIS-IV |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 101.090, 101.090, 148.600 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 30.000 - 2.000 |
R-factor | 0.173 |
Rwork | 0.173 |
R-free | 0.19800 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1oi2 |
RMSD bond length | 0.013 |
RMSD bond angle | 1.662 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 2.040 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.080 | 0.450 |
Number of reflections | 59910 | |
<I/σ(I)> | 22.6 | 6.88 |
Completeness [%] | 100.0 | 100 |
Redundancy | 12.38 | 10.95 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | 0.15 M DL-MALIC ACID PH 7.0, 20% PEG-3350 |