2IPT
PFA1 Fab Fragment
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 113 |
Detector technology | IMAGE PLATE |
Collection date | 2006-03-27 |
Detector | RIGAKU RAXIS IV |
Wavelength(s) | 1.54 |
Spacegroup name | P 1 |
Unit cell lengths | 41.985, 42.825, 58.381 |
Unit cell angles | 95.84, 94.77, 91.91 |
Refinement procedure
Resolution | 25.190 - 2.000 |
R-factor | 0.18 |
Rwork | 0.177 |
R-free | 0.22300 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2iq9 |
RMSD bond length | 0.011 |
RMSD bond angle | 1.429 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.190 | 2.070 |
High resolution limit [Å] | 2.000 | 2.000 |
Number of reflections | 25317 | |
Completeness [%] | 93.1 | 85.1 |
Redundancy | 1.9 | 1.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7.5 | 294 | 0.1 M Hepes, 25% PEG3350, pH 7.5, VAPOR DIFFUSION, temperature 294K |