2INY
Nanoporous Crystals of Chicken Embryo Lethal Orphan (CELO) Adenovirus Major Coat Protein, Hexon
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 298 |
Detector technology | IMAGE PLATE |
Detector | RIGAKU RAXIS II |
Spacegroup name | P 3 2 1 |
Unit cell lengths | 157.770, 157.770, 114.200 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 47.060 - 3.900 |
Rwork | 0.372 |
R-free | 0.41600 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1p30 |
RMSD bond length | 0.014 |
RMSD bond angle | 1.300 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.970 |
High resolution limit [Å] | 3.900 | 3.900 |
Number of reflections | 14636 | |
<I/σ(I)> | 7.1 | 2.5 |
Completeness [%] | 95.7 | 94.4 |
Redundancy | 4.6 | 4.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 295 | 7% iso-propanol, 13% PEG 4000, 0.01 M glycine, 0.1 M Hepes, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 295.0K |