2IK2

Yeast inorganic pyrophosphatase variant D115E with magnesium and phosphate

Refinement Statistics

Experimental method:X-RAY DIFFRACTION (1.8 Å)

Cell axes51.57893.36669.797
Cell angles90.0099.8690.00
SpacegroupP 1 21 1
Resolution limits19.88 - 1.80
the highest resolution shell value1.846 - 1.799
R-factor0.17728
R-work0.17518
the highest resolution shell value0.293
R-free0.21652
the highest resolution shell value0.304
RMSD bond length0.016
RMSD bond angle1.565

Data Collection Statistics

Resolution limits50.00 - 1.80
the highest resolution shell value -
Number of reflections58354
Rmerge_l_obs0.067
the highest resolution shell value0.344
Completeness96.8
Redundancy3.2
I/sigma(I)0

Crystallization Conditions

crystal IDmethodpHpH rangetemperatureunit
1VAPOR DIFFUSION6277

Crystallization Reagents

IDcrystal IDsolution IDreagent nameconcentrationdetails
Crystallization Reagents in Literatures*
IDcrystal IDsolutionreagent nameconcentration (unit)details
Annotated Information is extracted from Literature Info*