2IJG
Crystal Structure of cryptochrome 3 from Arabidopsis thaliana
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-06-10 |
Detector | ADSC QUANTUM 1 |
Wavelength(s) | 0.97926 |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 117.897, 117.897, 216.567 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 50.000 - 2.100 |
Rwork | 0.238 |
R-free | 0.26190 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1np7 |
RMSD bond length | 0.006 |
RMSD bond angle | 1.490 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASES |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 2.100 |
Rmerge | 0.200 |
Number of reflections | 52546 |
<I/σ(I)> | 14.6 |
Completeness [%] | 100.0 |
Redundancy | 10.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.4 | 294 | pH 6.4, VAPOR DIFFUSION, HANGING DROP, temperature 294K |