2I5K
Crystal structure of Ugp1p
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-11-13 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 0.979350 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 110.191, 147.437, 167.752 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.990 - 3.100 |
Rwork | 0.226 |
R-free | 0.29100 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1z90 |
RMSD bond length | 0.014 |
RMSD bond angle | 1.444 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 110.978 | 84.180 | 3.270 |
High resolution limit [Å] | 3.100 | 9.800 | 3.100 |
Rmerge | 0.102 | 0.080 | 0.286 |
Total number of observations | 3133 | 14948 | |
Number of reflections | 24806 | ||
<I/σ(I)> | 3.9 | 6.6 | 2.5 |
Completeness [%] | 98.9 | 93.5 | 100 |
Redundancy | 4.2 | 3.9 | 4.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.4 | 293 | 6% PEG-4000, 15-18% glycerol, 140mM Mg-formate, pH 7.4, VAPOR DIFFUSION, HANGING DROP, temperature 293K |