2I1Q
RadA Recombinase in complex with Calcium
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CLSI BEAMLINE 08ID-1 |
Synchrotron site | CLSI |
Beamline | 08ID-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-08-03 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 1.3303 |
Spacegroup name | P 61 |
Unit cell lengths | 84.200, 84.200, 104.700 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 20.000 - 1.900 |
R-factor | 0.191 |
Rwork | 0.191 |
R-free | 0.21100 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1xu4 |
RMSD bond length | 0.005 |
RMSD bond angle | 1.180 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | AMoRE |
Refinement software | CNS (1.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 2.090 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.062 | 0.420 |
Number of reflections | 31855 | |
<I/σ(I)> | 42.4 | 8.7 |
Completeness [%] | 99.7 | 99.4 |
Redundancy | 22.2 | 22 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.4 | 294 | 6% PEG 3350, 0.05M Tris-HCl, 0.005M MgCl2, 0.025M CaCl2, 0.002M ANP, pH 7.40, VAPOR DIFFUSION, HANGING DROP, temperature 294K |