2I1L
Crystal structure of the C2 form of FAD synthetase from Thermotoga maritima
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 5.0.2 |
Synchrotron site | ALS |
Beamline | 5.0.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2001-05-02 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 0.9795 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 95.187, 117.647, 79.270 |
Unit cell angles | 90.00, 126.79, 90.00 |
Refinement procedure
Resolution | 14.580 - 2.500 |
R-factor | 0.238 |
Rwork | 0.238 |
R-free | 0.28100 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1mrz |
RMSD bond length | 0.008 |
RMSD bond angle | 1.500 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 15.000 | 2.650 |
High resolution limit [Å] | 2.500 | 2.500 |
Number of reflections | 51065 | |
Completeness [%] | 97.7 | 97 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 298 | 0.2 mM sodium citrate, 10% polyethylene glycol 4000 (PEG4K), 5% glycerol, and 10% propanol, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |