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2HZ9

Crystal structure of Lys12Val/Asn95Val/Cys117Val mutant of human acidic fibroblast growth factor at 1.70 angstrom resolution.

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 22-BM
Synchrotron siteAPS
Beamline22-BM
Temperature [K]103
Detector technologyCCD
Collection date2006-07-17
DetectorMARMOSAIC 225 mm CCD
Wavelength(s)1
Spacegroup nameC 2 2 21
Unit cell lengths76.280, 95.370, 107.330
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution43.580 - 1.700
Rwork0.199
R-free0.22600
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1jqz
RMSD bond length0.012
RMSD bond angle1.600
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwareCNS
Refinement softwareCNS
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]43.5801.760
High resolution limit [Å]1.7001.700
Rmerge0.076
Number of reflections38559
<I/σ(I)>44.78
Completeness [%]90.699.6
Redundancy9
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP7.5298.15Ammonium Sulfate, Sodium Formate, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 298.15K

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