2HX1
Crystal structure of possible sugar phosphatase, HAD superfamily (ZP_00311070.1) from CYTOPHAGA HUTCHINSONII ATCC 33406 at 2.10 A resolution
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-2 |
Synchrotron site | SSRL |
Beamline | BL9-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-06-18 |
Detector | MARMOSAIC 325 mm CCD |
Wavelength(s) | 0.97932, 0.91837, 0.97915 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 65.624, 119.462, 151.274 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.323 - 2.100 |
R-factor | 0.18146 |
Rwork | 0.179 |
R-free | 0.23400 |
Structure solution method | MAD |
RMSD bond length | 0.016 |
RMSD bond angle | 1.433 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | SHELX |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 29.323 | 29.320 | 2.150 |
High resolution limit [Å] | 2.100 | 9.390 | 2.100 |
Rmerge | 0.152 | 0.045 | 0.635 |
Total number of observations | 2772 | 18914 | |
Number of reflections | 70192 | ||
<I/σ(I)> | 4.4 | 11.1 | 1.2 |
Completeness [%] | 100.0 | 96.6 | 100 |
Redundancy | 3.7 | 3.2 | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION,SITTING DROP,NANODROP | 7.5 | 277 | 15.0% Ethanol, 0.2M MgCl2, 0.1M HEPES pH 7.5, VAPOR DIFFUSION,SITTING DROP,NANODROP, temperature 277K |