2HJN
Structural and functional analysis of Saccharomyces cerevisiae Mob1
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X8C |
Synchrotron site | NSLS |
Beamline | X8C |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-04-01 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.9795, 0.9792, 0.9600 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 72.750, 70.811, 50.622 |
Unit cell angles | 90.00, 119.35, 90.00 |
Refinement procedure
Resolution | 35.000 - 2.000 |
R-factor | 0.20421 |
Rwork | 0.202 |
R-free | 0.23747 |
Structure solution method | MAD |
RMSD bond length | 0.020 |
RMSD bond angle | 1.760 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | SHARP |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 2.050 | |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.068 | 0.278 |
Number of reflections | 14415 | |
<I/σ(I)> | 18.4 | 2.9 |
Completeness [%] | 99.5 | 95 |
Redundancy | 5.3 | 3.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 277 | 1.2M ammonium sulfate, 0.1M MES, pH 6.0, VAPOR DIFFUSION, HANGING DROP, temperature 277K |