2HCF
Crystal structure of hydrolase haloacid dehalogenase-like family (np_662590.1) from Chlorobium tepidum TLS at 1.80 A resolution
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-2 |
Synchrotron site | SSRL |
Beamline | BL9-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-06-05 |
Detector | MARMOSAIC 325 mm CCD |
Wavelength(s) | 0.91837, 0.97915, 0.97929 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 37.750, 71.590, 83.200 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 27.951 - 1.800 |
R-factor | 0.192 |
Rwork | 0.189 |
R-free | 0.24700 |
Structure solution method | MAD |
RMSD bond length | 0.015 |
RMSD bond angle | 1.366 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 27.951 | 1.860 | |
High resolution limit [Å] | 1.800 | 3.070 | 1.800 |
Rmerge | 0.069 | 0.044 | 0.477 |
Number of reflections | 21098 | ||
<I/σ(I)> | 8.1 | 14.4 | 1.6 |
Completeness [%] | 92.2 | 98.1 | 72.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP, NANODROP | 8.5 | 277 | 0.2M MgCl2, 30.0% PEG-4000, 0.1M TRIS, pH 8.5, VAPOR DIFFUSION, SITTING DROP, NANODROP, temperature 277K |