2H8E
Structure RusA D70N
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-04-04 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.954 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 60.153, 85.107, 57.514 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 37.000 - 1.200 |
R-factor | 0.18315 |
Rwork | 0.183 |
R-free | 0.19132 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1q8r |
RMSD bond length | 0.007 |
RMSD bond angle | 1.197 |
Data scaling software | CCP4 ((SCALA)) |
Phasing software | MOLREP |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 37.000 | 1.260 |
High resolution limit [Å] | 1.200 | 1.200 |
Rmerge | 0.182 | |
Number of reflections | 36704 | |
Completeness [%] | 83.4 | 45 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 298 | 20% PEG 3350, 0.2M Sodium Tartrate, 0.1M Tris, pH 8.0, VAPOR DIFFUSION, HANGING DROP, temperature 298K |