2H8B
Solution structure of INSL3
Spectrometer
Experimental method: SOLUTION NMR
| Spectrometer ID | Spectrometer maker | Spectrometer model | Spectrometer type | Spectrometer field strength |
| 1 | Bruker | DMX | 750 | |
| 2 | Bruker | AVANCE | 600 |
Experiment
| experiment id | conditions id | solution id | Experiment type |
| 1 | 1 | 1 | 2D TOCSY |
| 10 | 2 | 2 | 2D TOCSY |
| 11 | 3 | 1 | 2D TOCSY |
| 12 | 3 | 1 | 2D NOESY |
| 13 | 3 | 2 | 2D NOESY |
| 14 | 3 | 2 | 2D TOCSY |
| 15 | 4 | 1 | 2D TOCSY |
| 16 | 4 | 1 | 2D NOESY |
| 17 | 4 | 2 | 2D NOESY |
| 18 | 4 | 2 | 2D TOCSY |
| 19 | 5 | 1 | 2D TOCSY |
| 2 | 1 | 1 | 2D NOESY |
| 20 | 5 | 1 | 2D NOESY |
| 21 | 5 | 2 | 2D NOESY |
| 22 | 5 | 2 | 2D TOCSY |
| 23 | 6 | 1 | 2D TOCSY |
| 24 | 6 | 1 | 2D NOESY |
| 25 | 6 | 2 | 2D NOESY |
| 26 | 6 | 2 | 2D TOCSY |
| 3 | 1 | 1 | DQF-COSY |
| 4 | 1 | 2 | 2D NOESY |
| 5 | 1 | 2 | 2D TOCSY |
| 6 | 1 | 2 | DQF-COSY |
| 7 | 2 | 1 | 2D TOCSY |
| 8 | 2 | 1 | 2D NOESY |
| 9 | 2 | 2 | 2D NOESY |
NMR Sample
| conditions id | NMR sample pH | NMR sample pressure | NMR sample temperature |
| 1 | 4 | ambient | 298 |
| 2 | 4 | ambient | 303 |
| 3 | 4 | ambient | 290 |
| 4 | 2.7 | ambient | 298 |
| 5 | 5.1 | ambient | 298 |
| 6 | 6.1 | ambient | 298 |
Conformers
| Conformers Calculated Total Number | 50 |
| Conformers Submitted Total Number | 20 |
