2H5F
Denmotoxin: A the three-finger toxin from colubrid snake Boiga dendrophila with bird-specific activity
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID29 |
| Synchrotron site | ESRF |
| Beamline | ID29 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2004-11-16 |
| Detector | ADSC QUANTUM 210 |
| Wavelength(s) | 1.006768 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 98.910, 34.038, 54.377 |
| Unit cell angles | 90.00, 118.36, 90.00 |
Refinement procedure
| Resolution | 47.670 - 1.900 |
| R-factor | 0.20373 |
| Rwork | 0.202 |
| R-free | 0.23840 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.032 |
| RMSD bond angle | 2.088 |
| Data scaling software | HKL-2000 |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.1.24) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 52.000 | 1.740 |
| High resolution limit [Å] | 1.700 | 1.700 |
| Number of reflections | 50240 | |
| Completeness [%] | 93.5 | 72.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 7.9 | 291 | 1.2M Na, KPO4, pH 7.9, VAPOR DIFFUSION, SITTING DROP, temperature 291K |
