2H4P
Crystal structure of wildtype MENT in the cleaved conformation
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 14-BM-C |
Synchrotron site | APS |
Beamline | 14-BM-C |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2003-11-24 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 1.000 |
Spacegroup name | P 1 |
Unit cell lengths | 46.486, 47.526, 57.794 |
Unit cell angles | 96.89, 93.81, 116.65 |
Refinement procedure
Resolution | 30.000 - 1.700 |
R-factor | 0.192 |
Rwork | 0.191 |
R-free | 0.21400 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1hle |
RMSD bond length | 0.005 |
RMSD bond angle | 0.805 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 1.760 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.040 | 0.159 |
Number of reflections | 40805 | |
<I/σ(I)> | 21.2 | |
Completeness [%] | 85.2 | 51 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 290 | 15% PEG 8000, 0.1M sodium cacodylate, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 290K |