2H1X

Crystal structure of 5-hydroxyisourate Hydrolase (formerly known as TRP, Transthyretin Related Protein)

Refinement Statistics

Experimental method:X-RAY DIFFRACTION (1.98 Å)

Cell axes58.07864.13558.937
Cell angles90.0094.0090.00
SpacegroupP 1 21 1
Resolution limits58.82 - 1.98
the highest resolution shell value2.031 - 1.980
R-factor0.20809
R-work0.20570
the highest resolution shell value0.184
R-free0.25168
the highest resolution shell value0.317
RMSD bond length0.008
RMSD bond angle1.159

Data Collection Statistics

Resolution limits500.00 - 1.98
the highest resolution shell value -
Number of reflections26947
Rmerge_l_obs0.048
the highest resolution shell value0.190
Completeness89.1
Redundancy3.2
the highest resolution shell value2.9
I/sigma(I)0

Crystallization Conditions

crystal IDmethodpHpH rangetemperatureunit
1VAPOR DIFFUSION, SITTING DROP7.5277

Crystallization Reagents

IDcrystal IDsolution IDreagent nameconcentrationdetails
Crystallization Reagents in Literatures*
IDcrystal IDsolutionreagent nameconcentration (unit)details
Annotated Information is extracted from Literature Info*