2H0K
Crystal Structure of a Mutant of Rat Annexin A5
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | ELLIOTT GX-21 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2003-11-24 |
Detector | MARRESEARCH |
Wavelength(s) | 1.5418 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 51.108, 67.184, 112.313 |
Unit cell angles | 90.00, 94.79, 90.00 |
Refinement procedure
Resolution | 33.590 - 2.760 |
R-factor | 0.201 |
Rwork | 0.197 |
R-free | 0.26100 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1a8a |
RMSD bond length | 0.009 |
RMSD bond angle | 1.229 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | AMoRE |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 33.590 | 2.910 |
High resolution limit [Å] | 2.760 | 2.760 |
Number of reflections | 19089 | |
<I/σ(I)> | 5.3 | 2 |
Completeness [%] | 97.1 | 88.8 |
Redundancy | 3.2 | 2.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.4 | 293 | PEG 8000, CALCIUM ACETATE, SODIUM CACODYLATE, SODIUM AZIDE, PH 6.4, VAPOR DIFFUSION, HANGING DROP, TEMPERATURE 293.0K, pH 6.40 |