2GZD
Crystal Structure of Rab11 in Complex with Rab11-FIP2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE BM14 |
Synchrotron site | ESRF |
Beamline | BM14 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-12-06 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 0.97865 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 64.364, 91.149, 113.099 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.000 - 2.440 |
R-factor | 0.22886 |
Rwork | 0.226 |
R-free | 0.27888 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | Rab11 in complex with Rab11-FIP in the trigonal space group |
RMSD bond length | 0.020 |
RMSD bond angle | 1.974 |
Data scaling software | HKL-2000 |
Phasing software | AMoRE |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.530 |
High resolution limit [Å] | 2.440 | 2.440 |
Rmerge | 0.102 | 0.421 |
Number of reflections | 24064 | |
<I/σ(I)> | 8.8 | |
Completeness [%] | 99.7 | 98.5 |
Redundancy | 13 | 10 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 5 | 298 | Ammonium phosphate buffer, between 0.1 and 0.5 M concentration, VAPOR DIFFUSION, temperature 298K |