2GR7
Hia 992-1098
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-3 |
Synchrotron site | ESRF |
Beamline | ID14-3 |
Temperature [K] | 100 |
Wavelength(s) | 0.931 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 97.340, 56.296, 158.706 |
Unit cell angles | 90.00, 90.04, 90.00 |
Refinement procedure
Resolution | 20.000 - 2.300 |
R-factor | 0.226 |
Rwork | 0.226 |
R-free | 0.25200 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.012 |
RMSD bond angle | 1.401 |
Data scaling software | CCP4 ((SCALA)) |
Phasing software | SOLVE |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 20.000 |
High resolution limit [Å] | 2.300 |
Number of reflections | 38510 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 10 | 293 | 100 mM CHES, 12% PEG 4000 and 200 mM ammonium sulfate, VAPOR DIFFUSION, HANGING DROP, temperature 293K |