2GON
Xray Structure of Gag133-278
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-2 |
Synchrotron site | SSRL |
Beamline | BL9-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 1999-05-31 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.97895, 0.97858, 0.94002 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 106.260, 134.509, 42.086 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.800 - 1.900 |
R-factor | 0.20493 |
Rwork | 0.202 |
R-free | 0.25713 |
Structure solution method | MAD |
RMSD bond length | 0.024 |
RMSD bond angle | 1.783 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SOLVE |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.800 | 1.949 |
High resolution limit [Å] | 1.900 | 1.900 |
Number of reflections | 48798 | |
Completeness [%] | 99.9 | 100 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 286 | 0.2 M BiAmmonium Citrate, 20% PEG 3350, pH 8.0, VAPOR DIFFUSION, SITTING DROP, temperature 286K |