2GO7
CRYSTAL STRUCTURE OF A HYDROLASE FROM HALOACID DEHALOGENASE-LIKE FAMILY (SP_2064) FROM STREPTOCOCCUS PNEUMONIAE TIGR4 AT 2.10 A RESOLUTION
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL11-1 |
Synchrotron site | SSRL |
Beamline | BL11-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-12-19 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.979224, 0.918370, 0.978940 |
Spacegroup name | P 61 |
Unit cell lengths | 155.000, 155.000, 88.440 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 29.290 - 2.100 |
R-factor | 0.173 |
Rwork | 0.171 |
R-free | 0.20900 |
Structure solution method | MAD |
RMSD bond length | 0.017 |
RMSD bond angle | 1.439 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | SHARP |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 29.480 | 2.170 | |
High resolution limit [Å] | 2.100 | 3.590 | 2.100 |
Rmerge | 0.085 | 0.053 | 0.521 |
Number of reflections | 70459 | 13699 | 10654 |
<I/σ(I)> | 6.83 | 13.4 | 1.55 |
Completeness [%] | 99.3 | 99.2 | 96.2 |
Redundancy | 3.76 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP, NANODROP | 5.5 | 277 | 0.2M MgCl2, 40.0% PEG-400, 0.1M Citrate, pH 5.5, VAPOR DIFFUSION, SITTING DROP, NANODROP, temperature 277K |