Experimental procedure
Spacegroup name | C 1 2 1 |
Unit cell lengths | 76.080, 27.780, 42.000 |
Unit cell angles | 90.00, 102.70, 90.00 |
Refinement procedure
Resolution | ? - 2.300 |
R-factor | 0.217 * |
Rwork | 0.217 |
RMSD bond length | 0.040 |
RMSD bond angle | 0.176 |
Refinement software | PROLSQ |
Data quality characteristics
Overall | |
High resolution limit [Å] | 2.300 * |
Total number of observations | 8747 * |
Number of reflections | 3905 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion * | 7.6 * | referred to J.Mol.Biol. 106.1077-1081 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 15 (mg/ml) | |
2 | 1 | drop | Tris-HCl | 0.05 (M) | |
3 | 1 | drop | PEG4000 | 20 (%) | |
4 | 1 | reservoir | PEG4000 | 10 (%) |