Experimental procedure
Spacegroup name | P 21 21 21 |
Unit cell lengths | 47.520, 59.060, 126.290 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 10.000 - 2.400 |
R-factor | 0.235 |
Rwork | 0.235 |
RMSD bond length | 0.013 |
RMSD bond angle | 22.500 * |
Phasing software | X-PLOR (3.1) |
Refinement software | X-PLOR (3.1) |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 4 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 10 (mg/ml) | |
2 | 1 | drop | potassium phosphate | 2 (mM) | |
3 | 1 | reservoir | PEG8000 | 21 (%(w/v)) | |
4 | 1 | reservoir | sodium citrate/phosphate | 0.2 (M) |