2GJG
CRYSTAL STRUCTURE OF A PILZ-CONTAINING PROTEIN (PP4397) FROM PSEUDOMONAS PUTIDA KT2440 AT 2.25 A RESOLUTION
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-2 |
Synchrotron site | SSRL |
Beamline | BL9-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-02-20 |
Detector | MARMOSAIC 325 mm CCD |
Wavelength(s) | 0.97941, 0.97879, 0.91162 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 89.224, 48.819, 57.476 |
Unit cell angles | 90.00, 93.41, 90.00 |
Refinement procedure
Resolution | 28.690 - 2.250 |
R-factor | 0.20976 |
Rwork | 0.206 |
R-free | 0.27500 |
Structure solution method | MAD |
RMSD bond length | 0.014 |
RMSD bond angle | 1.501 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | SOLVE |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 28.690 | 28.690 | 2.310 |
High resolution limit [Å] | 2.250 | 10.060 | 2.250 |
Rmerge | 0.061 | 0.023 | 0.300 |
Number of reflections | 11812 | ||
<I/σ(I)> | 8.8 | 27.7 | 1.2 |
Completeness [%] | 99.4 | ||
Redundancy | 3 | 2.8 | 2.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5.5 | 277 | 35.0% 2-propanol, 5.0% PEG-1000, 0.1M Citrate pH 5.5 , VAPOR DIFFUSION,SITTING DROP,NANODROP, temperature 277K |