2GJ2
Crystal Structure of VP9 from White Spot Syndrome Virus
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | NSLS BEAMLINE X12C |
| Synchrotron site | NSLS |
| Beamline | X12C |
| Temperature [K] | 298 |
| Detector technology | CCD |
| Collection date | 2004-10-12 |
| Detector | ADSC QUANTUM 4 |
| Wavelength(s) | 1.7 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 74.133, 78.205, 78.979 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 45.000 - 2.350 |
| Rwork | 0.225 |
| R-free | 0.27500 |
| Structure solution method | SAD |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.700 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | SOLVE |
| Refinement software | CNS (1.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 2.350 |
| High resolution limit [Å] | 2.270 | 2.270 |
| Number of reflections | 38474 | |
| Completeness [%] | 97.4 | 78.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6.3 | 298 | 2M sodium acetate, 100mM MES, 25mM cadmium sulfate, 3% glycerol, pH 6.3, VAPOR DIFFUSION, HANGING DROP, temperature 298K |
