2GIM
1.6 Angstrom structure of plastocyanin from Anabaena variabilis
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | MAX II BEAMLINE I711 |
Synchrotron site | MAX II |
Beamline | I711 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-10-25 |
Detector | MARRESEARCH |
Wavelength(s) | 1.11 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 67.850, 45.810, 63.410 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.190 - 1.600 |
R-factor | 0.21138 |
Rwork | 0.209 |
R-free | 0.26021 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | : 1BAW |
RMSD bond length | 0.018 |
RMSD bond angle | 1.859 |
Data scaling software | XDS |
Phasing software | MOLREP |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 1.800 |
High resolution limit [Å] | 1.550 | 1.550 |
Number of reflections | 24943 | |
Completeness [%] | 93.3 | 99.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 300 | 1.15 M trisodium citrate, 7.67 mM sodium borate buffer pH 8.5 , VAPOR DIFFUSION, SITTING DROP, temperature 300K |