2GGT
Crystal structure of human SCO1 complexed with nickel.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-11-30 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 0.97625 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 51.461, 52.444, 136.411 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 36.740 - 2.400 |
R-factor | 0.22562 |
Rwork | 0.217 |
R-free | 0.31793 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1wp0 |
RMSD bond length | 0.037 |
RMSD bond angle | 2.920 |
Data scaling software | CCP4 ((SCALA)) |
Phasing software | MOLREP |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 78.200 | 2.530 |
High resolution limit [Å] | 2.400 | 2.400 |
Rmerge | 0.092 | 0.455 |
Number of reflections | 14686 | |
<I/σ(I)> | 6.8 | 1.6 |
Completeness [%] | 97.1 | 81.5 |
Redundancy | 5.2 | 3.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 298 | 0.1 Tris-HCl, 25% PEG6000, pH 8.5, VAPOR DIFFUSION, SITTING DROP, temperature 298K |