2GGA
CP4 EPSP synthase liganded with S3P and Glyphosate
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU300 |
Temperature [K] | 90 |
Detector technology | IMAGE PLATE |
Collection date | 2005-10-17 |
Detector | RIGAKU RAXIS IV |
Wavelength(s) | 1.5418 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 63.086, 44.979, 77.251 |
Unit cell angles | 90.00, 106.45, 90.00 |
Refinement procedure
Resolution | 15.000 - 1.700 |
R-factor | 0.158 |
Rwork | 0.158 |
R-free | 0.18400 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2gg6 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.630 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 15.000 | 1.740 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.070 | 0.377 |
Number of reflections | 44653 | |
<I/σ(I)> | 29.3 | 4.6 |
Completeness [%] | 99.3 | 97.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 290 | (NH4)2SO4 / KCl / PEG 400 / HEPES-Na , pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 290K |