2GEL
2.05A crystal structure of Salmonella typhimurium YeaZ, form B
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-2 |
Synchrotron site | ESRF |
Beamline | ID14-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-09-20 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.93300 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 144.199, 83.658, 41.260 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.000 - 2.050 |
R-factor | 0.22 |
Rwork | 0.195 |
R-free | 0.22700 |
Structure solution method | MAD |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.100 |
High resolution limit [Å] | 2.050 | 2.050 |
Number of reflections | 29954 | |
Completeness [%] | 94.0 | 84 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |