2GBY
Structure of QacR Multidrug Transcriptional Regulator Bound to Bivalent Diamidine Berenil
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 4.2.2 |
Synchrotron site | ALS |
Beamline | 4.2.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-06-06 |
Detector | NOIR-1 |
Wavelength(s) | 1.078 |
Spacegroup name | P 42 21 2 |
Unit cell lengths | 171.340, 171.340, 94.530 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.000 - 2.900 |
R-factor | 0.2487 |
Rwork | 0.249 |
R-free | 0.29000 |
Structure solution method | FOURIER SYNTHESIS |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | CNS |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 3.000 |
High resolution limit [Å] | 2.900 | 2.900 |
Rmerge | 0.080 | 0.308 |
Number of reflections | 31538 | |
<I/σ(I)> | 12.1 | 3.8 |
Completeness [%] | 99.4 | 9.4 |
Redundancy | 5.82 | 5.65 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.7 | 298 | 3M ammonium sulfate and 1M sodium acetate, pH 4.7, VAPOR DIFFUSION, HANGING DROP, temperature 298K |