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2G9Y

Structure of S102T E. coli alkaline phosphatase in presence of phosphate at 2.00 A resolution

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU RU200
Temperature [K]93
Detector technologyIMAGE PLATE
Collection date2003-12-24
DetectorRIGAKU RAXIS IV
Wavelength(s)1.5418
Spacegroup nameI 2 2 2
Unit cell lengths76.460, 164.490, 192.530
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution32.700 - 2.000
R-factor0.205
Rwork0.205
R-free0.24200
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1y6v
RMSD bond length0.005
RMSD bond angle1.330
Data reduction softwared*TREK
Data scaling softwared*TREK
Phasing softwareCNS
Refinement softwareCNS
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]32.7002.070
High resolution limit [Å]2.0002.000
Rmerge0.0860.346
Number of reflections81030
<I/σ(I)>9.2
Completeness [%]98.697.8
Redundancy3.573.49
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP9.52932.0M ammonium sulfate, 100mM Tris, 10mM magnesium chloride, 0.01mM zinc chloride, pH 9.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K

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