2G9B
NMR solution structure of CA2+-loaded calbindin D28K
Spectrometer
Experimental method: SOLUTION NMR
| Spectrometer ID | Spectrometer maker | Spectrometer model | Spectrometer type | Spectrometer field strength |
| 1 | Varian | INOVA | 800 | |
| 2 | Varian | INOVA | 600 |
Experiment
| experiment id | conditions id | solution id | Experiment type |
| 1 | 2 | 1 | 4D_13C/15N-separated_NOESY |
| 2 | 2 | 2 | 4D_13C/13C-separated_NOESY |
| 3 | 1 | 3 | 3D_CT_13C_methyl-separated_NOESY |
| 4 | 2 | 3 | (4,2)D_CT_13C/13C_methyl-separated_NOESY |
| 5 | 1 | 3 | 4D_13C/15N-separated_NOESY |
| 6 | 2 | 3 | (4,2)D_13C/15N-separated_NOESY |
| 7 | 1 | 4 | 4D_15N/15N-separated_NOESY |
| 8 | 2 | 1 | (4,2)D_13C_ali/13C_aro-separated_NOESY |
NMR Sample
| conditions id | NMR sample pH | NMR sample pressure | NMR sample temperature |
| 1 | 7 | AMBIENT | 298 |
| 2 | 6.2 | AMBIENT | 323 |
Conformers
| Conformers Calculated Total Number | 900 |
| Conformers Submitted Total Number | 10 |
