2G84
Cytidine and deoxycytidylate deaminase zinc-binding region from Nitrosomonas europaea.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-08-24 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.97956 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 38.354, 73.789, 110.370 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 36.900 - 1.400 |
R-factor | 0.1299 |
Rwork | 0.128 |
R-free | 0.16040 |
Structure solution method | SAD |
RMSD bond length | 0.014 |
RMSD bond angle | 1.536 |
Data scaling software | SCALEPACK |
Phasing software | SHELXD |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 36.900 | 1.430 |
High resolution limit [Å] | 1.400 | 1.400 |
Rmerge | 0.061 | 0.317 |
Number of reflections | 54643 | |
<I/σ(I)> | 43 | 3.82 |
Completeness [%] | 86.8 | 41.4 |
Redundancy | 13.1 | 4.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 291 | 0.2 M magnesium chloride, 25% PEG 3350, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 291K |