2G7R
X-ray structure of the death domain of the human mucosa associated lymphoid tissue lymphoma translocation protein 1
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 19-BM |
| Synchrotron site | APS |
| Beamline | 19-BM |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2005-11-30 |
| Detector | SBC-3 |
| Wavelength(s) | 0.979 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 86.937, 88.910, 34.598 |
| Unit cell angles | 90.00, 113.45, 90.00 |
Refinement procedure
| Resolution | 19.800 - 2.700 |
| R-factor | 0.23807 |
| Rwork | 0.236 |
| R-free | 0.28417 |
| Structure solution method | SAD |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.565 |
| Data reduction software | HKL-2000 |
| Data scaling software | SCALEPACK |
| Phasing software | SOLVE |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 19.791 | 2.800 |
| High resolution limit [Å] | 2.700 | 2.700 |
| Rmerge | 0.130 | 0.269 |
| Number of reflections | 6562 | |
| <I/σ(I)> | 18 | 4 |
| Completeness [%] | 98.6 | 99.8 |
| Redundancy | 1.8 | 1.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 298 | VAPOR DIFFUSION, SITTING DROP, temperature 298.0K |
