2G4T
anomalous substructure of porcine pancreatic elastase (Na)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | EMBL/DESY, HAMBURG BEAMLINE X12 |
Synchrotron site | EMBL/DESY, Hamburg |
Beamline | X12 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-01-01 |
Detector | MARRESEARCH |
Wavelength(s) | 2.00 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 49.920, 57.660, 74.380 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.000 - 2.150 |
R-factor | 0.1573 |
Rwork | 0.156 |
R-free | 0.23896 |
Structure solution method | FOURIER SYNTHESIS |
RMSD bond length | 0.023 |
RMSD bond angle | 1.791 |
Data reduction software | DENZO |
Data scaling software | CCP4 ((SCALA)) |
Phasing software | FFT |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 30.000 |
High resolution limit [Å] | 2.150 |
Number of reflections | 12156 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |