2G4Q
Anomalous substructure of lysozyme at pH 8.0
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | EMBL/DESY, HAMBURG BEAMLINE X12 |
Synchrotron site | EMBL/DESY, Hamburg |
Beamline | X12 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-01-01 |
Detector | MARRESEARCH |
Wavelength(s) | 2.00 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 77.170, 77.170, 37.050 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.000 - 1.840 |
R-factor | 0.16786 |
Rwork | 0.167 |
R-free | 0.20613 |
Structure solution method | FOURIER SYNTHESIS |
RMSD bond length | 0.020 |
RMSD bond angle | 1.730 |
Data reduction software | DENZO |
Data scaling software | CCP4 ((SCALA)) |
Phasing software | FFT |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 30.000 |
High resolution limit [Å] | 1.840 |
Number of reflections | 10159 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |