2G4M

Insulin collected at 2.0 A wavelength

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	EMBL/DESY, HAMBURG BEAMLINE X12
Synchrotron site	EMBL/DESY, HAMBURG
Beamline	X12
Temperature [K]	100
Detector technology	CCD
Collection date	2005-01-01
Detector	MARRESEARCH
Wavelength(s)	2.00
Spacegroup name	I 21 3
Unit cell lengths	78.270, 78.270, 78.270
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	30.000 - 1.800
R-factor	0.1677
Rwork	0.167
R-free	0.22295
Structure solution method	FOURIER SYNTHESIS
RMSD bond length	0.025
RMSD bond angle	1.777
Data reduction software	DENZO
Data scaling software	CCP4 ((SCALA))
Phasing software	FFT
Refinement software	REFMAC (5.2.0005)

Data quality characteristics

	Overall
Low resolution limit [Å]	30.000
High resolution limit [Å]	1.800
Number of reflections	7537

Crystallization Conditions

crystal ID	method	pH	temperature	details
1