2FZ1
Structure of Empty Head Turnip Yellow Mosaic Virus (ATC) at 100 K
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 5.0.2 |
Synchrotron site | ALS |
Beamline | 5.0.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 1998-12-11 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 1.0 |
Spacegroup name | P 64 2 2 |
Unit cell lengths | 511.360, 511.360, 304.310 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 48.640 - 2.900 |
R-factor | 0.309 |
Rwork | 0.309 |
R-free | 0.31500 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1auy |
RMSD bond length | 0.010 |
RMSD bond angle | 1.600 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.530 | 2.940 |
High resolution limit [Å] | 2.890 | 2.890 |
Number of reflections | 281901 | |
<I/σ(I)> | 4.37 | 0.41 |
Completeness [%] | 63.2 | 21.5 |
Redundancy | 3.35 | 1.15 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.4 | 298 | 1.0-1.7 M NH4PO4, 0.1 M MES buffer, pH 4.4, VAPOR DIFFUSION, HANGING DROP, temperature 298K |