2FUA
L-FUCULOSE 1-PHOSPHATE ALDOLASE CRYSTAL FORM T WITH COBALT
Experimental procedure
Detector technology | AREA DETECTOR |
Collection date | 1994 |
Detector | SIEMENS-NICOLET X100 |
Spacegroup name | P 4 21 2 |
Unit cell lengths | 93.700, 93.700, 42.800 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 10.000 - 2.000 |
R-factor | 0.18 |
Rwork | 0.180 |
RMSD bond length | 0.013 |
RMSD bond angle | 1.700 |
Data reduction software | XDS |
Phasing software | X-PLOR (3.0) |
Refinement software | X-PLOR (3.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 10.000 * | |
High resolution limit [Å] | 2.000 * | 2.000 * |
Rmerge | 0.061 | 0.159 * |
Number of reflections | 15207 | |
Completeness [%] | 89.0 * | 80 * |
Redundancy | 2.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 7.6 * | 293 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 10 (mg/ml) | |
2 | 1 | drop | Tris-HCl | 20 (mM) | |
3 | 1 | drop | 0.5 (mM) | ||
4 | 1 | drop | beta-mercaptoethanol | 10 (mM) | |
5 | 1 | reservoir | ammonium sulfate | 1.62 (M) | |
6 | 1 | reservoir | potassium phosphate | 20 (mM) | |
7 | 1 | reservoir | 4 (mM) | ||
8 | 1 | reservoir | beta-mercaptoethanol | 4 (mM) |