2FSY
Bacteriophage HK97 Pepsin-treated Expansion Intermediate IV
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL11-1 |
Synchrotron site | SSRL |
Beamline | BL11-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-05-31 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.181 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 1006.394, 1006.394, 728.693 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.000 - 3.800 |
Rwork | 0.337 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ohg |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.870 |
High resolution limit [Å] | 3.800 | 3.800 |
Rmerge | 0.170 | 0.425 |
Number of reflections | 2144154 | 48089 |
<I/σ(I)> | 5.5 | 1.8 |
Completeness [%] | 59.9 | 44.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.2 | 293 | 100mM Sodium Citrate pH 3.5, 400mM Magnesium Acetate Hexahydrate, 25% 1,6-Hexanediol, pH 5.2, vapor diffusion, hanging drop, temperature 293K |
1 | VAPOR DIFFUSION, HANGING DROP | 5.2 | 293 | 100mM Sodium Citrate pH 3.5, 400mM Magnesium Acetate Hexahydrate, 25% 1,6-Hexanediol, pH 5.2, vapor diffusion, hanging drop, temperature 293K |