2FR5
Crystal Structure of Mouse Cytidine Deaminase Complexed with Tetrahydrouridine
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL26B2 |
Synchrotron site | SPring-8 |
Beamline | BL26B2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-05-23 |
Detector | RIGAKU JUPITER 210 |
Wavelength(s) | 0.9 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 82.238, 93.403, 180.743 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 41.490 - 1.480 |
R-factor | 0.169 |
Rwork | 0.168 |
R-free | 0.19000 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1mq0 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.447 |
Data reduction software | BBS |
Data scaling software | d*TREK (8.0SSI) |
Phasing software | MOLREP |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 41.490 | 1.530 |
High resolution limit [Å] | 1.480 | 1.480 |
Rmerge | 0.073 | 0.288 |
Total number of observations | 73184 | |
Number of reflections | 111799 | 11283 |
<I/σ(I)> | 15.6 | 5 |
Completeness [%] | 96.7 | 98.9 |
Redundancy | 6.63 | 5.26 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4 | 298 | 0.8M AMMONIUM SULPHATE, 0.1M CITRATE, pH 4.0, VAPOR DIFFUSION, HANGING DROP, temperature 298.0K |